3-formyl-N,N-dimethylbenzene-1-sulfonamide → 4-Formyl-N-methylbenzenesulfonamide

HRID 333037노트

반응식

HRID 333037 반응식
C([C:3]1[CH:4]=[C:5]([S:9]([N:12]([CH3:14])C)(=[O:11])=[O:10])[CH:6]=[CH:7][CH:8]=1)=O.C(NS(C1C=CC=C([CH:27]=[O:28])C=1)(=O)=O)C.C(C1C=C(S(NCCC)(=O)=O)C=CC=1)=O.C(C1C=C(S(NC(C)C)(=O)=O)C=CC=1)=O>>[CH:27]([C:8]1[CH:3]=[CH:4][C:5]([S:9]([NH:12][CH3:14])(=[O:10])=[O:11])=[CH:6][CH:7]=1)=[O:28]

참가 물질

5

반응물 4

HCID 198159763-formyl-N,N-dimethylbenzene-1-sulfonamideHCID 86676515N-ethyl-3-formyl-benzenesulfonamideHCID 866765163-formyl-N-propyl-benzenesulfonamideHCID 866765173-formyl-N-isopropyl-benzenesulfonamide

생성물 1

HCID 143271774-Formyl-N-methylbenzenesulfonamide

실험 절차

3-Formyl-N,N-dimethyl-benzenesulfonamide, N-ethyl-3-formyl-benzenesulfonamide, 3-formyl-N-propyl-benzenesulfonamide and 3-formyl-N-isopropyl-benzenesulfonamide were oils and were used without further purification in the next step of reaction.

후처리

  1. customwere used without further purification in the next step of reaction

출처 및 근거

ORD 기록
ord-44f48bbac74f4f55ae5d2c5966139bb6
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08877946B2

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