2-Iodoaniline → 4-(3-(2-Iodophenyl)thioureido)benzenesulfonamide

반응식

[N:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]([NH2:13])(=[O:12])=[O:11])=[CH:6][CH:5]=1)=[C:2]=[S:3].[I:14][C:15]1[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=1[NH2:17]>>[I:14][C:15]1[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=1[NH:17][C:2](=[S:3])[NH:1][C:4]1[CH:5]=[CH:6][C:7]([S:10]([NH2:13])(=[O:11])=[O:12])=[CH:8][CH:9]=1

참가 물질

반응물 2

HCID 119952-Iodoaniline

HCID 5213594-Isothiocyanatobenzenesulfonamide

생성물 1

HCID 204092794-(3-(2-Iodophenyl)thioureido)benzenesulfonamide

실험 절차

The subject compound was prepared utilizing the procedure described above from 4-isothiocyanatobenzenesulfonamide and 2-iodoaniline. 1H NMR (400 MHz, DMSO-d6) δ 10.16 (s, 1H), 9.60 (s, 1H), 7.90-7.81 (m, 8H), 7.76 (bs, 2H); (M+H)+ (434).

후처리

customThe subject compound was prepared

출처 및 근거

ORD 기록: ord-b8ff775a343442dea1083eb2ec6797fd
출처 데이터셋: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08877970B2

반응 노트

불러오는 중…