2-Iodoaniline → HCID 57773639, 화합물

HRID 333121노트

반응식

HRID 333121 반응식
[N:1]([C:4]1[CH:5]=[C:6]([S:10]([NH2:13])(=[O:12])=[O:11])[CH:7]=[CH:8][CH:9]=1)=[C:2]=[S:3].[I:14][C:15]1[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=1[NH2:17]>>[I:14][C:15]1[CH:21]=[CH:20][CH:19]=[CH:18][C:16]=1[NH:17][C:2](=[S:3])[NH:1][C:4]1[CH:5]=[C:6]([S:10]([NH2:13])(=[O:11])=[O:12])[CH:7]=[CH:8][CH:9]=1

참가 물질

3

반응물 2

HCID 119952-IodoanilineHCID 100361773-isothiocyanatobenzenesulfonamide

생성물 1

HCID 57773639HCID 57773639, 화합물

실험 절차

The subject compound was prepared utilizing the procedure described above from 3-isothiocyanatobenzenesulfonamide and 2-iodoaniline. 1H NMR (400 MHz, DMSO-d6) δ 10.07 (s, 1H), 9.52 (s, 1H), 8.01-7.37 (m, 9H), 7.04 (m, 1H); (M+H)+ (434).

후처리

  1. customThe subject compound was prepared

출처 및 근거

ORD 기록
ord-e14082f72f6d43209f89e848dc6cb3c2
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08877970B2

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