Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Fluoro-3-nitrobenzotrifluoride → Tert-butyl [3-methyl-3-(2-nitro-4-trifluoromethyl-phenylamino)-butyl]-carbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Fluoro-3-nitrobenzotrifluoride | HCID 67778 | — |
| 반응물 | tert-butyl N-(3-amino-3-methylbutyl)carbamate | HCID 45072486 | — |
| 생성물 | Tert-butyl [3-methyl-3-(2-nitro-4-trifluoromethyl-phenylamino)-butyl]-carbamate | HCID 86603968 | — |
반응 단계
This is prepared analogously to method 2a) from a total of 3.25 g (15.5 mmol) 1-fluoro-2-nitro-4-trifluoromethyl-benzene and 2.74 g (13.5 mmol) tert-butyl (3-amino-3-methyl-butyl)-carbamate. 6.1 g yellow oil. Mass spectroscopy: [M+H]+=392.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07429583B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-466c0b33939342febed166262092aff5 |
| 출처 메모 | uspto-grants-2008_09 |