Oxalyl chloride → HCID 86688296, 화합물
반응식
[CH3:1][O:2][C:3]1[N:8]=[C:7]([C:9]([OH:11])=O)[CH:6]=[CH:5][CH:4]=1.C(Cl)(=O)C([Cl:15])=O>C(Cl)Cl>[CH3:1][O:2][C:3]1[N:8]=[C:7]([C:9]([Cl:15])=[O:11])[CH:6]=[CH:5][CH:4]=1참가 물질
4
반응 조건
- 온도
- 40 °C
실험 절차
To a mixture of 5.00 g (32.7 mmol) 6-methoxy-pyridine-2-carboxylic acid in 100 mL DCM was added 40.8 mL (81.6 mmol) 2 M oxalyl chloride solution in DCM and stirred at 40° C. for 2 h. The solvent was removed by distillation.
후처리
- customThe solvent was removed by distillation
출처 및 근거
- ORD 기록
- ord-7a3cb02637e540c3acfd20ff7e0b5407
- 출처 데이터셋
- uspto-grants-2014_11
- 특허 번호
- US08883789B2
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