Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Nitrofuroyl chloride → 5-nitro-N-[2-(piperidin-1-yl)phenyl]furan-2-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Nitrofuroyl chloride | HCID 90711 | — |
| 반응물 | 2-(Piperidin-1-yl)aniline | HCID 458795 | — |
| 생성물 | 5-nitro-N-[2-(piperidin-1-yl)phenyl]furan-2-carboxamide | HCID 2995620 | 100% |
반응 단계
The compound was prepared according to the procedure described in Example 2 from 5-nitro-furan-2-carbonyl chloride and 2-piperidinoaniline. Yield: 100%. MS: 316 (M+1). LC/MS purity: 100%. 1HNMR (CDCl3, 300 MHz): δ 8.2 (d, 1H), 7.85 (d, 1H), 7.55 (m, 1H), 7.4 (m, 3H), 3.8-3.2 (bm, 4H), 2.7-1.9 (bm, 6H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07429603B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-a048a0ae055d459d856eeafc414d3f81 |
| 출처 메모 | uspto-grants-2008_09 |