Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 335409생성일: 2026년 10월 23일
Triethylamine → 1-[2-(2,6-Diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-(1-methylethylidene)hydrazine
https://huagongshe.com/ko/reaction/335409
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 2-Propanone, methylhydrazone | HCID 79840 | — |
| 반응물 | 2-(2,6-Diethyl-4-methylphenyl)-2-oxoacetyl chloride | HCID 56942712 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 1-[2-(2,6-Diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-(1-methylethylidene)hydrazine | HCID 86689343 | — |
반응 단계
To a 1000 ml volume four-necked flask, 1-methyl-2-(2-propylidene)hydrazine (17-a) (9.61 g), acetonitrile (280 ml), and triethylamine (17 ml) were added under a nitrogen atmosphere and cooled to about 1° C. To the mixture, 2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl chloride (6-a) (27.12 g) dissolved in acetonitrile (77 ml) was added dropwise over 30 minutes.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08884010B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_11 |
|---|
| ORD ID | ord-32796de4843940589233da3d6cd68bbe |
|---|
| 출처 메모 | uspto-grants-2014_11 |
|---|
