Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
8-Amino-2-naphthalenol → 8-(1-Phenethyl-5-(trifluoromethyl)-1H-benzo[d]imidazol-2-ylamino)naphthalen-2-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 8-Amino-2-naphthalenol | HCID 8358 | — |
| 반응물 | 2-Chloro-1-phenethyl-5-(trifluoromethyl)-1H-benzo[d]imidazole | HCID 69200704 | — |
| 생성물 | 8-(1-Phenethyl-5-(trifluoromethyl)-1H-benzo[d]imidazol-2-ylamino)naphthalen-2-ol | HCID 11626508 | — |
반응 단계
The reaction of 2-chloro-1-phenethyl-5-(trifluoromethyl)-1H-benzo[d]imidazole from step (b) above (98 mg, 0.3 mol) with 8-amino-naphthalen-2-ol (64 mg, 0.2 mmol, Aldrich) under the condition of Example 21(b) afforded the title compound. MS (ESI, pos. ion) m/z: 448(M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07429608B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-fe9eb6c536f14fcf872702c51c7dd0ca |
| 출처 메모 | uspto-grants-2008_09 |