Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Thioglycolate → Methyl 7-chlorobenzo[b]thiophene-2-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Thioglycolate | HCID 16907 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 3-Chloro-2-fluorobenzaldehyde | HCID 736335 | — |
| 생성물 | Methyl 7-chlorobenzo[b]thiophene-2-carboxylate | HCID 22474203 | — |
반응 단계
Using 1.0 g (6.31 mmol) of 2-fluoro-3-chlorobenzaldehyde, 0.38 g (9.46 mmol) of sodium hydride (60% pure) and 0.74 g (6.94 mmol) of methyl mercaptoacetate, 1.04 g (72.3% of theory) of the title compound are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08884017B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-4405c32f1aac44f9a2a3c72a256429e2 |
| 출처 메모 | uspto-grants-2014_11 |