Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Anthranilamide → 2-[4-(4-Oxidanylidene-3h-Quinazolin-2-Yl)phenoxy]ethanoic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Anthranilamide | HCID 6942 | — |
| 반응물 | Acetic acid, 2-(4-formylphenoxy)- | HCID 89177 | — |
| 반응물 | 5,7-dimethoxy-2-(pyridin-2-yl)quinazolin-4(3H)-one | HCID 136037998 | — |
| 생성물 | 2-[4-(4-Oxidanylidene-3h-Quinazolin-2-Yl)phenoxy]ethanoic Acid | HCID 135566659 | 73% |
반응 단계
2-(4-(4-Oxo-3,4-dihydroquinazolin-2-yl)phenoxy)acetic acid was synthesized from anthranilamide and 4-formyl phenoxy acetic acid, using the method described for 5,7-dimethoxy-2-(pyridin-2-yl)quinazolin-4(3H)-one. 2-(4-(4-Oxo-3,4-dihydroquinazolin-2-yl)phenoxy)acetic acid (800 mg, 73%) was isolated as a white solid. Selected data: MS (m/z): 296.98; MP 285-287° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08889698B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-0723a2b089064791b68c9f6968fce0ec |
| 출처 메모 | uspto-grants-2014_11 |