Benzaldehyde → 1-(1h-Benzo[d]imidazol-5-yl)-5-phenylimidazolidine-2,4-dione

HRID 336816

반응식

[NH2:1][C:2]1[CH:10]=[CH:9][C:5]2[N:6]=[CH:7][NH:8][C:4]=2[CH:3]=1.[CH:11](=[O:18])C1C=CC=CC=1.[CH2:19]([N+]#[C-])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1.[O:28]([C:30]#[N:31])[K]>>[NH:6]1[C:5]2[CH:9]=[CH:10][C:2]([N:1]3[CH:19]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=4)[C:30](=[O:28])[NH:31][C:11]3=[O:18])=[CH:3][C:4]=2[N:8]=[CH:7]1

참가 물질

반응물 4

HCID 240Benzaldehyde

HCID 136235-Aminobenzimidazole

HCID 82558Benzyl isocyanide

HCID 178418250HCID 178418250, 화합물

생성물 1

HCID 1785185301-(1h-Benzo[d]imidazol-5-yl)-5-phenylimidazolidine-2,4-dione

실험 절차

The compound was synthesized starting from 5-aminobenzimidazole 1.331 g (10 mmol), benzaldehyde 1.02 ml (10 mmol), benzyl isonitrile 1.22 ml (10 mmol) and KOCN 0.84 g (10 mmol) as described in method 1.

후처리

customThe compound was synthesized

출처 및 근거

ORD 기록: ord-ca3e553280d0453991f068f1985dcf57
출처 데이터셋: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08889709B2

연결된 노트

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