Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Fluoro-2-nitrophenol → 2-Amino-4-fluorophenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Fluoro-2-nitrophenol | HCID 136236 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Amino-4-fluorophenol | HCID 2735917 | 86.9% |
반응 단계
300 mg of 4-fluoro-2-nitrophenol was dissolved in 3 ml of ethanol, and 120 mg of 10% palladium/carbon was added and stirred under hydrogen atmosphere at room temperature for 1 hour. After the insoluble matter was filtered off, the filtrate was distilled off under reduced pressure to yield 211 mg of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08889727B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-3bdbe08535b049f4b504bdb13705ee74 |
| 출처 메모 | uspto-grants-2014_11 |