Acetylacetone → 4-(3,5-dimethyl-1H-pyrazol-1-yl)-3-hydroxyphenyl acetate

HRID 337360

반응식

HRID 337360 반응식
C[C:2]1[CH:7]=[CH:6]C(S(O)(=O)=O)=[CH:4][CH:3]=1.[C:12]([O:15][C:16]1[CH:21]=[CH:20][C:19]([NH:22][NH2:23])=[C:18]([OH:24])[CH:17]=1)(=[O:14])[CH3:13].C(OC1C=CC(N)=C(O)C=1)(=O)C.C(CC(=O)C)(=O)C>>[C:12]([O:15][C:16]1[CH:21]=[CH:20][C:19]([N:22]2[C:7]([CH3:6])=[CH:2][C:3]([CH3:4])=[N:23]2)=[C:18]([OH:24])[CH:17]=1)(=[O:14])[CH3:13]

참가 물질

4

실험 절차

330 mg of the title compound was prepared in a manner similar to Example 54b) by using 4-hydrazinyl-3-hydroxyphenyl acetate 4-methylbenzenesulfonate (0.9 g), which was prepared from 4-amino-3-hydroxyphenyl acetate (1.0 g) in a manner similar to Example 54a), and acetylacetone (0.9 g).

출처 및 근거

ORD 기록
ord-2c512ac043bc473fbfb08611a07be3b5
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08889727B2

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