(1S*,2R*)-2-(1-Ethyl-1H-pyrazol-5-yl)cyclopentanol → HCID 89962477, 화합물

HRID 337919

반응식

HRID 337919 반응식
[CH2:1]([N:3]1[C:7]([C@H:8]2[CH2:12][CH2:11][CH2:10][C@@H:9]2[OH:13])=[CH:6][CH:5]=[N:4]1)[CH3:2]>CCCCCC.C(O)C>[CH2:1]([N:3]1[C:7]([C@@H:8]2[CH2:12][CH2:11][CH2:10][C@H:9]2[OH:13])=[CH:6][CH:5]=[N:4]1)[CH3:2]

참가 물질

3

반응물 1

HCID 89962858(1S*,2R*)-2-(1-Ethyl-1H-pyrazol-5-yl)cyclopentanol

생성물 1

HCID 89962477HCID 89962477, 화합물

시약·촉매·용매 1

HCID 21879635Ethanol hexane용매

실험 절차

The (1S*,2R*)-2-(1-ethyl-1H-pyrazol-5-yl)cyclopentanol prepared in Example 37a was optically resolved with CHIRALPAK AD-H (Daicel Corp.; hexane/ethanol=8:2) to yield the title compound as a colorless oil.

출처 및 근거

ORD 기록
ord-4f23d62afb48461dbab7291e5b9b4d86
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08889741B2

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