Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → HCID 178420610, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | 2,6-Diformylpyridine | HCID 79485 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178420610 | HCID 178420610 | — |
반응 단계
2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07429684B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-21efaacccac443d7a83aa3e70255ab54 |
| 출처 메모 | uspto-grants-2008_09 |