1,3-Benzodioxole-5-carboxylic acid → N-(1-hydroxypentan-2-yl)benzo[d][1,3]dioxole-5-carboxamide

HRID 339325

반응식

HRID 339325 반응식
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([OH:12])=O)=[CH:9][C:4]=2[O:3][CH2:2]1.[NH2:13][CH:14]([CH2:17][CH2:18][CH3:19])[CH2:15][OH:16]>>[OH:16][CH2:15][CH:14]([NH:13][C:10]([C:8]1[CH:7]=[CH:6][C:5]2[O:1][CH2:2][O:3][C:4]=2[CH:9]=1)=[O:12])[CH2:17][CH2:18][CH3:19]

참가 물질

3

반응물 2

HCID 71961,3-Benzodioxole-5-carboxylic acidHCID 2490172-Amino-1-pentanol

생성물 1

HCID 66775475N-(1-hydroxypentan-2-yl)benzo[d][1,3]dioxole-5-carboxamide수율 76%

실험 절차

N-(1-hydroxypentan-2-yl)benzo[d][1,3]dioxole-5-carboxamide was prepared in a similar manner to example 4 using benzo[d][1,3]dioxole-5-carboxylic acid and 2-aminopentan-1-ol. Yield: 76%. MS (M+H, 252).

출처 및 근거

ORD 기록
ord-3294ed54ce0f4bd9b23ed4931a51294d
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08895050B2

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