4-Heptanamine → HCID 57527950, 화합물

HRID 339332

반응식

HRID 339332 반응식
[O:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[CH:3]=[C:2]1[C:10](Cl)=[O:11].[CH3:13][CH2:14][CH2:15][CH:16]([NH2:20])[CH2:17][CH2:18][CH3:19]>>[CH2:15]([CH:16]([NH:20][C:10]([C:2]1[O:1][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[CH:3]=1)=[O:11])[CH2:17][CH2:18][CH3:19])[CH2:14][CH3:13]

참가 물질

3

반응물 2

HCID 386654-HeptanamineHCID 389492-Benzofurancarbonyl chloride

생성물 1

HCID 57527950HCID 57527950, 화합물수율 73%

실험 절차

Prepared in a similar manner to example 1 using benzofuran-2-carbonyl chloride and heptan-4-amine. Yield: 73%. 1H NMR (500 MHz, CDCl3): δ 0.93 (t, 6H, J=7.2 Hz), 1.41 (m, 8H), 3.01 (s, 3H), 4.18 (m, 1H), 6.29 (d, 1H, J=9.94 Hz), 7.20 (d, 1H, J=8.62 Hz), 7.37 (m, 2H), 7.44 (s, 1H). MS (M+H, 260)

출처 및 근거

ORD 기록
ord-c778a30032254e9bb6ee13027b06b310
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08895050B2

연결된 노트

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