4-Heptanamine → 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide

HRID 339340

반응식

HRID 339340 반응식
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[OH:11])[C:5]([OH:7])=O.[CH3:12][CH2:13][CH2:14][CH:15]([NH2:19])[CH2:16][CH2:17][CH3:18]>>[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[OH:11])[C:5]([NH:19][CH:15]([CH2:16][CH2:17][CH3:18])[CH2:14][CH2:13][CH3:12])=[O:7]

참가 물질

3

반응물 2

HCID 386654-HeptanamineHCID 650833-Amino-4-hydroxybenzoic acid

생성물 1

HCID 667731203-amino-4-hydroxy-N-(1-propylbutyl)benzamide수율 57%

실험 절차

3-amino-4-hydroxy-N-(1-propylbutyl)benzamide was prepared in a similar manner to example 4 using 3-Amino-4-hydroxybenzoic acid and 4-heptylamine. Yield 57%. 1H NMR (500 MHz, CDCl3): δ 0.93 (t, 6H); 1.26-1.51 (m, 8H); 4.09 (m, 1H); 6.74 (m, 1H); 7.05 (s, 1H); 7.43 (m, 2H); 7.77 (m, 2H). MS: (251, M+H).

출처 및 근거

ORD 기록
ord-2e3ce0e3ec9140c6a2db21225c34d2f5
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08895050B2

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