Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1,1-Trimethoxy-2-chloroethane → Chloromethyl benzooxazol-5-carboxylic acid (1-propyl-butyl)amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1,1-Trimethoxy-2-chloroethane | HCID 144702 | — |
| 반응물 | 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide | HCID 66773120 | — |
| 생성물 | Chloromethyl benzooxazol-5-carboxylic acid (1-propyl-butyl)amide | HCID 57331139 | 65% |
반응 단계
Prepared in a similar manner to example 41 using 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide (example 41a) and trimethyl chloro-orthoacetate. Yield: 65%. mp 108.5-109° C. MS (M+H, 309.05).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08895050B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-9ff0e655b215451087923139b829be0e |
| 출처 메모 | uspto-grants-2014_11 |