Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cycloheptylamine → N-cycloheptyl-2,3,5,6-tetrafluoro-4-methylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cycloheptylamine | HCID 2899 | — |
| 반응물 | p-Toluic acid, 2,3,5,6-tetrafluoro- | HCID 69548 | — |
| 생성물 | N-cycloheptyl-2,3,5,6-tetrafluoro-4-methylbenzamide | HCID 57527795 | — |
반응 단계
Prepared in a similar manner to Example 162 using cycloheptylamine and 2,3,5,6-tetrafluoro-p-toluic acid (94%). 1H NMR (CDCl3) δ 1.53 (m, 6H), 1.57 (m, 4H), 2.03 (m, 2H) 2.28 (m, 3H), 4.17 (m, 1H), 5.85 (bs, 1H). MS (304.1, M+H) m. p. 164-165° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08895050B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-58c2686c0d494547812b9bd9d5356594 |
| 출처 메모 | uspto-grants-2014_11 |