Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 6-[(3,5-Diacetylphenyl)amino]purine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Cni H1894 | HCID 463010 | — |
| 반응물 | 6-Chloropurine | HCID 5359277 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 6-[(3,5-Diacetylphenyl)amino]purine | HCID 12093260 | 90.4% |
반응 단계
Compound No. 16: A suspension of 3,5-diacetylaniline (0.531 g) in water (10 mL) was treated with 6-chloropurine (0.464 g) and concentrated HCl (0.25 mL) and heated at reflux for 30 min. After cooling the mixture was treated with 6 mL of aqueous 1N KOH. The mixture was stirred for 10 min and the solid was filtered out, washed with water, and dried, to give 0.80 g of 6-[(3,5-diacetylphenyl)amino]purine, mp dec 340°-350° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05733932 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-0b3c68dde58a4f4fbcd3c8750233eef7 |
| 출처 메모 | uspto-grants-1998_03 |