Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline → 4-Acetoxy-N-[4-(6-methoxybenzothiazol-2-yl)-phenyl]-benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline | HCID 391870 | — |
| 반응물 | p-Acetoxybenzoyl chloride | HCID 2756254 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 4-Acetoxy-N-[4-(6-methoxybenzothiazol-2-yl)-phenyl]-benzamide | HCID 67312482 | 94.3% |
반응 단계
Prepared as described in the Amide Coupling section above using 2-(4-aminophenyl)-6-methoxybenzothiazole (0.25 g, 0.976 mmol) and 4-acetoxybenzoyl chloride (0.22 g, 1.07 mmol) in dry pyridine (10 ml) to give the title compound (0.385 g, 94%) as a colourless solid after work-up.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08895313B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-af2d3d64779f46498e30f8d105d55e59 |
| 출처 메모 | uspto-grants-2014_11 |