Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline → HCID 67313154, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline | HCID 391870 | — |
| 반응물 | 4-Methoxy-3-(trifluoromethyl)benzoyl chloride | HCID 2775298 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 67313154 | HCID 67313154 | 87% |
반응 단계
Prepared as described in the Amide Coupling section using 2-(4-aminophenyl)-6-methoxybenzothiazole (0.5 g, 1.95 mmol) and 4-methoxy-3-trifluoromethylbenzoyl chloride (0.47 g, 1.95 mmol) in dry pyridine (15 ml) to give the title compound (0.77 g, 87%) as pale yellow feathery crystals after work-up and recrystallisation from acetic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08895313B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-f231a315b48e409ca85777f2f217b6a9 |
| 출처 메모 | uspto-grants-2014_11 |