Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,2-Dimethoxypropane → (2,2-Dimethyl-1,3-dioxan-5-yl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,2-Dimethoxypropane | HCID 6495 | — |
| 반응물 | Methylpropanediol | HCID 75103 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | (2,2-Dimethyl-1,3-dioxan-5-yl)methanol | HCID 3584869 | — |
반응 단계
A solution of 2,2-dimethoxypropane (5.88 g, 56.5 mmol), 2-methyl-propane-1,3-diol (5.0 g, 47 mmol), and PTSA monohydrate (0.48 g, 2.3 mmol) in THF (100 mL) was stirred O/N at rt. The mixture was concentrated in vacuo to give the title compound as a colorless liquid: yield 6.87 g (99%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08895534B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-cfb4541aa01a4f7da4634bef9d0cf3d5 |
| 출처 메모 | uspto-grants-2014_11 |