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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 339647생성일: 2026년 10월 25일

Piperonal → Bis(3,4-methylenedioxy)chalcone

https://huagongshe.com/reaction/339647

반응식

참여 물질

역할이름HCID투입량
반응물PiperonalHCID 8438—
반응물Sodium HydroxideHCID 14798—
반응물AcetopiperoneHCID 76622—
용매EthanolHCID 702—
생성물Bis(3,4-methylenedioxy)chalconeHCID 294346—

반응 단계

A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08895554B2
출처 데이터셋uspto-grants-2014_11
ORD IDord-65bba51aa38742f684bf9a2217b6badf
출처 메모uspto-grants-2014_11