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[N:1]([C:4]1[CH:5]=[C:6](O)[CH:7]=[CH:8][CH:9]=1)=[N+:2]=[N-:3].NC1C=CC([OH:18])=CC=1>>[N:1]([C:4]1[CH:5]=[CH:6][C:7]([OH:18])=[CH:8][CH:9]=1)=[N+:2]=[N-:3]참가 물질
3
실험 절차
4-Azidophenol was prepared similarly to 3-azidophenol, using 4-aminophenol (5.0 g) instead of 3-aminophenol. This gave 5.27 g (85% yield) of a dark red oil. 1H NMR (acetone-d6, 300 MHz, ppm): 8.48 (s, 1H, Ar—OH), 6.94 (m, 4H, Ar—H). 13C NMR (MeOD-d4, 75 MHz, ppm): 156.4, 132.4, 121.1, 117.7. FT-IR (cm−1): 3372, 2113, 2072.
출처 및 근거
- ORD 기록
- ord-e9097652a1f841c189a8029ba99148e2
- 출처 데이터셋
- uspto-grants-2014_11
- 특허 번호
- US08895688B2
연결된 노트
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