Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-(Chlorocarbonyl)phenyl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Acetoxybenzoic acid | HCID 238669 | — |
| 생성물 | 3-(Chlorocarbonyl)phenyl acetate | HCID 12998558 | 99% |
반응 단계
Using the above procedure, reaction of with thionyl chloride (11.1 mL, 15.3 mmol) and 3-acetoxybenzoic acid (2.50 g, 13.9 mmol) gave 511 (2.72 g, 99%) as a colorless oil. This material was used in the next step without additional purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08895752B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-0532de99dffc4e219aa9a7c1fb11c578 |
| 출처 메모 | uspto-grants-2014_11 |