Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Sulfoxide → 2,3-Dihydro-1-benzofuran-7-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Sulfoxide | HCID 679 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | (2,3-Dihydro-1-benzofuran-7-yl)methanol | HCID 2795020 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 2,3-Dihydro-1-benzofuran-7-carbaldehyde | HCID 2795018 | 95.4% |
반응 단계
A solution of 2,3-dihydro-benzofuran-7-methanol (8.13 g, 54.5 mmol) was oxidized using DMSO, oxalyl chloride, and triethyl amine similar to the above procedures to give the product as an oil (7.7 g, 95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05856529 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-a852a7612a1547eda322c0ef871cb06e |
| 출처 메모 | uspto-grants-1999_01 |