Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,6-Dibromohexane → 6-[4-(6-Bromo-benzo[d]-isoxazol-3-yl)-phenoxy]-hexyl-methyl-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,6-Dibromohexane | HCID 12368 | — |
| 반응물 | N-Methylallylamine | HCID 69391 | — |
| 반응물 | 6-Bromo-3-[4-(6-bromo-hexyloxy)-phenyl]-benzo[d]isoxazole | HCID 67598318 | — |
| 반응물 | 4-(6-Bromo-benzo[d]isoxazol-3-yl)-phenol | HCID 136365325 | — |
| 생성물 | 6-[4-(6-Bromo-benzo[d]-isoxazol-3-yl)-phenoxy]-hexyl-methyl-amine | HCID 22446497 | — |
반응 단계
Analogously to Example 1, from 4-(6-bromo-benzo[d]isoxazol3-yl)-phenol and 1,6-dibromohexane via 6-bromo-3-[4-(6-bromo-hexyloxy)-phenyl]-benzo[d]isoxazole and by reaction with N-allyl-methyl-amine there is obtained allyl-[6-[4-(6-bromo-benzo[d]-isoxazol-3-yl)-phenoxy]-hexyl-methyl-amine which is converted into the fumarate, MS: m/e 442 (M+H+, 1 Br).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05856503 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-2e9c175a30694f62bf54fff62070ea29 |
| 출처 메모 | uspto-grants-1999_01 |