Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl bromide → 2-Propenyloxydibenzofuran
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2-Dibenzofuranol | HCID 66587 | — |
| 생성물 | 2-Propenyloxydibenzofuran | HCID 57252405 | — |
반응 단계
A solution of 2-hydroxydibenzofuran (2.0 grams) was treated with allyl bromide (1.2 mL) and potassium carbonate (1.5 grams). The mixture was stirred over night at 60°. The reaction was partitioned between methylene chloride and water. The organic was washed once with water and dried over sodium sulfate. The organic layer was filtered and concentrated to an oil which was chromatographed over silica gel to afford the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05859051 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-3e18335d1be24ab18925c6d52005670c |
| 출처 메모 | uspto-grants-1999_01 |