Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formamide → 4-(N-formylaminomethyl)benzophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formamide | HCID 713 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 4-(Chloromethyl)benzophenone | HCID 3016376 | — |
| 반응물 | Sodium Diformylamide | HCID 10877056 | — |
| 용매 | Sodium Methoxide | HCID 10942334 | — |
| 생성물 | 4-(N-formylaminomethyl)benzophenone | HCID 53721082 | — |
반응 단계
150 g of formamide are stirred together with 90 mL of 30%ig sodium methylate solution for 8 hours under slight vacuum at 80° C. To the resulting solution of sodium diformylamide there are added 150 g of 4-chloromethylbenzophenone. After 15 hours the suspension originally present has changed to a clear solution which is added to 1l of 10%ig sodium carbonate solution. A solid material precipitates, which is filtered off in vacuo and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05859084 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-f04bdcdffb864269893718aa61552b51 |
| 출처 메모 | uspto-grants-1999_01 |