Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → Ethyl 2-benzylideneaminobutyrate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Ethyl 2-Aminobutyrate Hydrochloride | HCID 12844023 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Ethyl 2-benzylideneaminobutyrate | HCID 10331026 | — |
반응 단계
Triethylamine (2 moles) was added to a solution of the product from step (a) (1 mole) in toluene. When addition was complete, benzaldehyde (1 mole) was added. The mixture was azeotroped until no further water was collected, then cooled to room temperature and filtered. The filtrate was evaporated in vacuo ti give the desired product as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05859240 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-410984a921a147c6bb9ce5296f537673 |
| 출처 메모 | uspto-grants-1999_01 |