반응식
[CH3:1][CH:2]([CH:6]([CH3:10])[C:7]([OH:9])=[O:8])[C:3](O)=[O:4].C(Cl)(=O)C>>[CH3:1][CH:2]1[CH:6]([CH3:10])[C:7](=[O:9])[O:8][C:3]1=[O:4]참가 물질
3
반응 조건
- 온도
- 65 °C
실험 절차
To the 2,3-dimethyl succinic acid (5.13 g, 35.1 mmol), was added acetyl chloride (8.27 g, 7.49 mL, 105 mmol) at room temperature. The reaction mixture was refluxed at about 65° C. for 2 hrs. Workup consisted of concentration in vacuo, and drying in high vacuo. The desired product (4.95 g, with a little impurity of acetic acid) was obtained as a white solid.
후처리
- concentrationWorkup consisted of concentration in vacuo
- customdrying in high vacuo
출처 및 근거
- ORD 기록
- ord-57939b2bc3864ae9a6026904999a5656
- 출처 데이터셋
- uspto-grants-1999_01
- 특허 번호
- US05861428
연결된 노트
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