돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 343469생성일: 2026년 10월 25일

N-[2-(3,4-Dichlorophenyl)-4-oxobutyl]-N-methylbenzamide → N-Methylbenzamide

https://huagongshe.com/reaction/343469

반응식

참여 물질

역할이름HCID투입량
반응물N-[2-(3,4-Dichlorophenyl)-4-oxobutyl]-N-methylbenzamideHCID 22137499—
반응물4-[(2,2,2-Trifluoroacetyl)[3-(2,2,2-trifluoroacetylamino)propyl]amino]piperidineHCID 22137527—
반응물(S)-N-[2-(3,4-Dichlorophenyl)-4-[4-[(2,2,2-trifluoro-acetyl)[2-(2,2,2-trifluoroacetylamino)ethyl]amino]piperidino]-butyl]-N-methylbenzamideHCID 54511194—
생성물N-MethylbenzamideHCID 11954—

반응 단계

(S)-N-[2-(3,4-Dichlorophenyl)-4-[4-[(2,2,2-trifluoroacetyl)-[2-(2,2,2-trifluoroacetylamino)ethyl]amino]piperidino]butyl]-N-methylbenzamide. Using the procedure of Example 1, replacing 4-(2-oxo-1,3-oxazolidin-3-yl)piperidine by 4-[(2,2,2-trifluoroacetyl)-[3-(2,2,2-trifluoroacetylamino)propyl]amino]piperidine, and N-[2-(3,4-dichlorophenyl)-4-oxobutyl]-N-methylbenzamide by the (S)-enantiomer, the N-methylbenzamide was obtained; MS: m/z=683(M+1).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05861392
출처 데이터셋uspto-grants-1999_01
ORD IDord-d4d3395435c54436a22020e92c14f88c
출처 메모uspto-grants-1999_01