Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → HCID 11436590, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 2,6-Xylyl isothiocyanate | HCID 87976 | — |
| 반응물 | N-Ethylglycine | HCID 316542 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 11436590 | HCID 11436590 | 18.4% |
반응 단계
A mixture of N-ethyl glycine (9.2 g), 2,6-dimethylphenyl-isothiocyanate (8.2 g), triethylamine (10.1 g), and methylene chloride (150 mL) was heated at reflux for 3.5 hours. The mixture was evaporated to dryness. Purification was achieved through crystallization from ethanol. The title compound (2.3 g) was obtained as a white solid (2.3 g). m.p. 128°-131° C. Anal. Calcd. for. C13H16N2OS: C, 62.87; H, 6.49; N, 11.28. Found: C, 62.83; H, 6.50; N, 11.25. Mass spectrum (EI, M.+) m/z 248.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05861517 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-497f500330044158bb46447d68ff46cf |
| 출처 메모 | uspto-grants-1999_01 |