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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 343615생성일: 2026년 10월 26일

Triethylamine → 1-Isopropyl-3-(2-isopropylphenyl)2-thioxo-imidazolidin-4-one

https://huagongshe.com/reaction/343615

반응식

참여 물질

역할이름HCID투입량
반응물TriethylamineHCID 8471—
반응물2-Isopropylphenyl isothiocyanateHCID 142052—
반응물NoName_76HCID 414244—
용매ChloroformHCID 6212—
생성물1-Isopropyl-3-(2-isopropylphenyl)2-thioxo-imidazolidin-4-oneHCID 8674979743.6%

반응 단계

The title compound was prepared by the procedure described in Example 18 using 10.0 g of 2-isopropylphenyl-isothiocyanate, 11.9 g of N-isopropyl glycine, 12.0 g of triethyl amine, and 200 mL of chloroform. Crystallization from ethanol afforded the title compound (6.8 g) as a light pink solid, m.p. 112°-114° C. Anal. Calcd. for. C15H20N2OS: C, 65.18; H, 7.29; N, 10.13. Found: C, 65.51; H, 7.25; N, 10.32. Mass spectrum (EI, M.+) m/z 276.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05861517
출처 데이터셋uspto-grants-1999_01
ORD IDord-42804dbe06c14569a567ce221e26f5a2
출처 메모uspto-grants-1999_01