Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → HCID 178525732, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Formic acid, copper salt | HCID 44152240 | — |
| 반응물 | HCID 178525731 | HCID 178525731 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 178525732 | HCID 178525732 | 40.5% |
반응 단계
2.58 g of 1,4-trans-cyclohexane dicarboxylic acid was dissolved under heating in a mixture solvent of 100 cm3 of methanol and 20 cm3 of formic acid. After this solution was cooled to the normal temperature, into this solution under stirring, a further solution in which 3.38 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 1.43 g of 1,4-trans-cyclohexane dicarboxylic acid copper was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05862796 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-c01f4852e5434038b46b74957eb732e9 |
| 출처 메모 | uspto-grants-1999_01 |