Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → 2,6-Naphthalene dicarboxylic acid copper
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | 2,6-Naphthalenedicarboxylic acid | HCID 14357 | — |
| 반응물 | Formic acid, copper salt | HCID 44152240 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2,6-Naphthalene dicarboxylic acid copper | HCID 69858079 | 67.6% |
반응 단계
0.40 g of 2,6-naphthalene dicarboxylic acid was dissolved under heating in a mixture solvent of 4000 cm3 of methanol and 5 cm3 of formic acid. After this solution was cooled to the normal temperature, into this solution under stirring, a further solution in which 3.00 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 0.35 g of 2,6-naphthalene dicarboxylic acid copper was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05862796 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-c4bbc6cb1fc74cb0907db7ff81c62b12 |
| 출처 메모 | uspto-grants-1999_01 |