Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-[4-Cyano-2-(2-phenylethynyl)phenyl]hydantoin → 5-[4-Cyano-2-(2-phenylethyl)phenyl]hydantoin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-[4-Cyano-2-(2-phenylethynyl)phenyl]hydantoin | HCID 70076578 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 5-[4-Cyano-2-(2-phenylethyl)phenyl]hydantoin | HCID 70074777 | — |
반응 단계
A solution of 5-[4-cyano-2-(2-phenylethynyl)phenyl]hydantoin (100 mg, 0.33 mmol) in methanol (20 ml) was shaken with 10% palladium-carbon (10 mg) under an atmosphere of hydrogen for 24 hours at 60 p.s.i. The catalyst was removed by filtration to give 5-[4-cyano-2-(2-phenylethyl)phenyl]hydantoin as a colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05863947 |
| 출처 데이터셋 | uspto-grants-1999_01 |
| ORD ID | ord-0ebda7467daf448680d696c08ef0e4de |
| 출처 메모 | uspto-grants-1999_01 |