Thiophenol → Benzene, [(6-bromohexyl)thio]-

HRID 344248노트

반응식

HRID 344248 반응식
[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(=O)([O-])[O-].[K+].[K+].[Br:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]Br>>[C:1]1([S:7][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][Br:14])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

4

반응물 3

HCID 7969ThiophenolHCID 11430Potassium CarbonateHCID 123681,6-Dibromohexane

생성물 1

HCID 10849841Benzene, [(6-bromohexyl)thio]-수율 99.5%

실험 절차

Thiophenol (3 g), potassium carbonate (5.64 g) and 1,6-dibromohexane (6.64 g) were reacted and treated in the same manner as in Preparation Example 99 to give 7.4 g of 6-phenylthiohexyl bromide.

후처리

  1. additiontreated in the same manner as in Preparation Example 99

출처 및 근거

ORD 기록
ord-ca68285e59d34206979c93e1ffc965a1
출처 데이터셋
uspto-grants-1999_01
특허 번호
US05864039

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