Glycinamide hydrochloride → Dimiracetam

HRID 344745

반응식

HRID 344745 반응식
Cl.[NH2:2][CH2:3][C:4]([NH2:6])=[O:5].[O:7]=[CH:8][CH2:9][CH2:10][C:11](OCC(C)C)=O>>[O:5]=[C:4]1[CH2:3][N:2]2[C:8](=[O:7])[CH2:9][CH2:10][CH:11]2[NH:6]1

참가 물질

3

반응물 2

HCID 2723639Glycinamide hydrochlorideHCID 10464575Isobutyl 4-oxobutanoate

생성물 1

HCID 65955Dimiracetam수율 22.6%

실험 절차

Glycinamide hydrochloride (4.2 g, 38 mmol) and isobutyl 4-oxobutanoate (5 g, 31.6 mmol) were reacted together according to the procedure of example 2, to give the title compound 1 g (22.6%), m.p. 154°-157° C.

출처 및 근거

ORD 기록
ord-743505df9dcc4cf8a94543234b8b5e8f
출처 데이터셋
uspto-grants-1991_10
특허 번호
US05053422

연결된 노트

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