Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → 9-Octadecenal, (9Z)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Oleyl Alcohol | HCID 5284499 | — |
| 반응물 | HCID 178418287 | HCID 178418287 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 9-Octadecenal, (9Z)- | HCID 5364492 | 90.1% |
반응 단계
An 18 g portion of pyridinium chlorochromate was slurried in 200 ml of dichloromethane. A solution of 15 g of oleyl alcohol in 200 ml of dichloromethane was added. This mixture was stirred for 4 hours, then poured into ether and filtered through hydrous magnesium silicate. The filtrate was evaporated, giving 13.42 g of the desired compound as a colorless liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05053426 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-0a27b92f0b3f46f8b3c80fea1702af49 |
| 출처 메모 | uspto-grants-1991_10 |