Dichloromaleic anhydride → N,N-bis-(3-chloroallyl) dichloromaleic monoamide
반응식
[Cl:1][C:2]1=[C:3]([Cl:9])[C:4]([O:6][C:7]1=[O:8])=[O:5].[Cl:10][CH:11]=[CH:12][CH2:13][NH:14][CH2:15][CH:16]=[CH:17][Cl:18]>C(Cl)Cl>[Cl:10][CH:11]=[CH:12][CH2:13][N:14]([CH2:15][CH:16]=[CH:17][Cl:18])[C:4](=[O:5])/[C:3](/[Cl:9])=[C:2](/[Cl:1])\[C:7]([OH:6])=[O:8]참가 물질
4
실험 절차
Dichloromaleic anhydride (1.7 g, 0.01 mol) and 30 ml methylene chloride were stirred under a mild reflux. Bis-(3-chloroallyl)amine (1.7 g, 0.01 mol) was then added. The exothermic reaction yielded a clear solution. The solution was stirred at room temperature for 3 hours. The mixture was stripped, resulting in 3.3 g of the above-named product.
후처리
- customThe exothermic reaction
- customyielded a clear solution
출처 및 근거
- ORD 기록
- ord-5050602a882a45ac90f3b09ce19acbb6
- 출처 데이터셋
- uspto-grants-1988_08
- 특허 번호
- US04762548
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