Methyl p-toluenesulfonate → HCID 86745141, 화합물

HRID 345197노트

반응식

HRID 345197 반응식
[CH3:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[CH3:12][O:13][S:14]([C:17]1[CH:22]=[CH:21][C:20]([CH3:23])=[CH:19][CH:18]=1)(=[O:16])=[O:15]>>[CH3:12][N+:3]1[C:4]2[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=2)[CH:10]=[CH:11][C:2]=1[CH3:1].[CH3:23][C:20]1[CH:21]=[CH:22][C:17]([S:14]([OH:16])(=[O:15])=[O:13])=[CH:18][CH:19]=1

참가 물질

3

반응물 2

HCID 6645Methyl p-toluenesulfonateHCID 70602-Methylquinoline

생성물 1

HCID 86745141HCID 86745141, 화합물

실험 절차

2-Methyl-quinoline (71.5 pbw) and methyl-p-toluenesulfonate (102.3 pbw) are heated for about 10 minutes at 100° C. An exothermic reaction sets in, in which the mixture is heated to 180.C. After another 10 minutes the mixture is poured onto acetone, filtered with suction, washed with acetone and dried.

후처리

  1. customAn exothermic reaction sets in, in which the mixture
  2. additionAfter another 10 minutes the mixture is poured onto acetone
  3. filtrationfiltered with suction
  4. washwashed with acetone
  5. customdried

출처 및 근거

ORD 기록
ord-d610caabd6674847a09a87c6df6e813e
출처 데이터셋
uspto-grants-1991_10
특허 번호
US05055579

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