Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1-Pyrrolidino-1-cyclohexene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Cyclohexanone | HCID 7967 | — |
| 반응물 | Pyrrolidine | HCID 31268 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 1-Pyrrolidino-1-cyclohexene | HCID 70768 | 95.9% |
반응 단계
Cyclohexanone (196.3 g) and pyrrolidine (214 g) in benzene (500 ml) were refluxed under nitrogen with a Dean-Stark apparatus, until no more water separated out. The solvents were then evaporated off under nitrogen, and the residual oil was distilled to give 1-(1-pyrrolidinyl)cyclohexene (290 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05057513 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-cf667839892a418383ce21ec62dc57f8 |
| 출처 메모 | uspto-grants-1991_10 |