Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 2-Benzylcyclohexan-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | 1-Cyclohexylpyrrolidine | HCID 139064 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 2-Benzylcyclohexan-1-one | HCID 98945 | — |
반응 단계
A mixture of 1-(1-pyrrolidinyl)cyclohexane (85.4 g) and benzyl chloride (100 ml) in dioxane (400 ml) was heated under reflux for 23 hours under nitrogen. Water (100 ml) was then added and the brown oil was distilled to give (2RS)-2-phenylmethylcyclohexanone (47.1 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05057513 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-21da1710588a4bcabd47799acedec4b2 |
| 출처 메모 | uspto-grants-1991_10 |