Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dibenzylhydroxylamine → N-tert-octyl-[3-(N,N-dibenzylaminoxy)-propionamide]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dibenzylhydroxylamine | HCID 69297 | — |
| 반응물 | N-tert-Octylacrylamide | HCID 171970 | — |
| 반응물 | Potassium tert-butoxide | HCID 23665647 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | N-tert-octyl-[3-(N,N-dibenzylaminoxy)-propionamide] | HCID 57149163 | — |
반응 단계
The procedure of Example I is repeated using 23.31 g of dibenzylhydroxylamine, 1.23 g of potassium-tert-butoxide and 20.0 g of N-tert-octylacrylamide in 100 ml of dry tetrahydrofuran to afford the title compound as a white crystalline solid: mp 96°-98° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05057563 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-5a98df59669f4e07a5cf00f6d0fde8ea |
| 출처 메모 | uspto-grants-1991_10 |