Diethylhydroxylamine → 3-[(Diethylamino)oxy]-N-(2,4,4-trimethylpentan-2-YL)propanamide

HRID 345516노트

반응식

HRID 345516 반응식
[CH2:1]([N:3]([CH2:5][CH3:6])[OH:4])[CH3:2].CC(C)([O-])C.[K+].[C:13]([NH:21][C:22](=[O:25])[CH:23]=[CH2:24])([CH2:16][C:17]([CH3:20])([CH3:19])[CH3:18])([CH3:15])[CH3:14]>O1CCCC1>[C:13]([NH:21][C:22](=[O:25])[CH2:23][CH2:24][O:4][N:3]([CH2:5][CH3:6])[CH2:1][CH3:2])([CH2:16][C:17]([CH3:18])([CH3:19])[CH3:20])([CH3:14])[CH3:15]

참가 물질

5

반응물 3

HCID 19463DiethylhydroxylamineHCID 171970N-tert-OctylacrylamideHCID 23665647Potassium tert-butoxide

생성물 1

HCID 569757343-[(Diethylamino)oxy]-N-(2,4,4-trimethylpentan-2-YL)propanamide

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The procedure of Example I is repeated using diethylhydroxylamine, potassium-tert-butoxide and N-tertoctylacrylamide in tetrahydrofuran to afford the title compound.

출처 및 근거

ORD 기록
ord-b59eae3428c2448b9904cc5861b64b11
출처 데이터셋
uspto-grants-1991_10
특허 번호
US05057563

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