Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → N,N-Dibenzyl-O-carbamylhydroxylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Dibenzylhydroxylamine | HCID 69297 | — |
| 반응물 | Potassium cyanate | HCID 11378442 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N,N-Dibenzyl-O-carbamylhydroxylamine | HCID 15180714 | — |
반응 단계
A stirred suspension of 10.70 g of N,N-dibenzylhydroxylamine in 25 ml of methanol is admixed dropwise with a solution of 4.53 ml conc. hydrochloric acid in 10 ml of water. A solution of 4.06 g of potassium cyanate in 15 ml of water is then added and the resulting suspension is stirred at room temperature for 3 hours. The crude product is removed by filtration and further purified by liquid chromatography to afford the title compound as a white solid; m.p. 127°-29° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05057610 |
| 출처 데이터셋 | uspto-grants-1991_10 |
| ORD ID | ord-c6e69c66052b4a1caae6615e35fa0218 |
| 출처 메모 | uspto-grants-1991_10 |