N,N-Dimethylethylenediamine → N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-N',N'-dimethylethylenediamine

HRID 34563

반응식

HRID 34563 반응식
[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[CH3:23][N:24]([CH3:28])[CH2:25][CH2:26][NH2:27]>>[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([NH:27][CH2:26][CH2:25][N:24]([CH3:28])[CH3:23])=[O:6]

참가 물질

3

반응물 2

HCID 66053N,N-DimethylethylenediamineHCID 1285703,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenic acid

생성물 1

HCID 53955451N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-N',N'-dimethylethylenediamine수율 88%

실험 절차

The procedure of Example 9 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 3.3 ml of N,N-dimethylethylene diamine were used as starting materials. 6.5 g (yield 88%) of the title compound was obtained as a pale yellow oil.

출처 및 근거

ORD 기록
ord-72725f58058848e5b39d0da2169d49e7
출처 데이터셋
uspto-grants-1988_08
특허 번호
US04762829

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